Bulk Anisic Acid Raw Materials powder

CAS:100-09-4

MF:C8H12N2

MW:136.19

EINECS:214-391-2

Specification: 99% min Anisic Acid

Sample:Anisic Acid powder Avaliable

Packaging:1kg/bag, 25kg/drum

Brand: Ausreson

Appearance:white powder

Storage: Cool Dry Place

Shelf Life: 2 Years

Test Method: HPLC

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Anisic Acid of Usage and Synthesis.

‌ Cosmetics and perfumery ‌ : p-methoxybenzoic acid is a white or colorless solid organic compound with a benzene ring attached to one methoxy group on one side and a carboxylic acid group on the other. It has certain aromatic and antibacterial, antioxidant effects, so it is widely used in the cosmetics and fragrance industry, such as perfume, soap, cosmetics, toothpaste and chewing gum and other products.

‌ pharmaceutical intermediate ‌ : low toxicity to methoxybenzoic acid, can irritate eyes, skin and mucous membranes. It is mainly used in pharmaceutical intermediates, as organic raw materials, preparation of flavors and flavors and general reagents ‌.

‌ Preservatives and pharmaceutical raw materials ‌ : Draconic Acid is used as a raw material for preservatives, medicines and fragrances. It has antibacterial and antiseptic activities, properties that make it potentially useful in medical and hygiene fields ‌.

‌ safety ‌ : methoxybenzoic acid should be packed with anti-static measures and stored in a cool, dry and well-ventilated warehouse, away from fire and heat sources. Keep containers sealed to avoid contamination and ensure safety.

Uses of Anisic Acid.

The metabolism of Aniracetam, a drug that models anti-anxiety behavior, Anisic Acid in cosmetics is also an inhibitor of tyrosinase. It is obtained by the reaction of p-hydroxybenzoic acid with dimethyl sulfate. It can also be used as a pharmaceutical intermediate such as solacetam and ethanesulfonone.

Multifunctional Cosmetic Agent.

Technical Specifications

Quality Standards Comparison

Industrial use of p-Anisic Acid.

Methyl anisate

Put anisic acid, methanol and concentrated sulfuric acid into a round-bottom flask in a certain molar ratio, install a spherical condenser, heat with a water bath, and reflux at 96-100°C. After the reaction is completed, remove the condenser and change it to a distillation device to evaporate the excess methanol.
When the residual liquid in the round-bottom flask is cooled to room temperature, neutralize it with a saturated sodium carbonate solution until the residual liquid is neutral. At this time, white crystalline methyl anisate precipitates, and filter it to obtain a crude product. The crude product is subjected to vacuum distillation, and the 160°C/20mrnHg fraction is collected to obtain a refined product.

Ethyl anisate

Put anisic acid, anhydrous ethanol, concentrated sulfuric acid and benzene into a round-bottom flask in a certain ratio, shake well, add zeolite, install a water separator, and connect a reflux spherical condenser to the upper end of the water separator. Heat the round-bottom flask with water latently and reflux at 96-100°C. After the reaction is completed, continue to heat with a water bath.
The excess benzene and ethanol were evaporated into the water separator. The residual liquid in the flask was cooled to room temperature, neutralized with saturated sodium carbonate to neutrality, and the oil layer was separated with a separatory funnel; the water layer was extracted with ether three times, the ether and the oil layer were combined, and dried with anhydrous magnesium carbonate for two hours. Afterwards, the ether was evaporated with a water bath, and then under reduced pressure, the 136-137°C/13mmHg fraction was collected to obtain ethyl anisate.

Product method of Bulk Anisic Acid Powder.

It is obtained by the reaction of p-hydroxybenzoic acid with dimethyl sulfate.

Medicinal effects of Anisic Acid Powder

Anisic acid is present in large quantities in fennel (fennel), which is also rich in vitamin C, a small amount of vitamin B2, lotus glycosides, fennel glycosides, cinnamic acid, caffeic acid, anisic acid and other organic acids. It has the effects of dispelling wind, dissipating heat, relieving gas and relieving pain. It is mainly used for cold hernia, stomach cold vomiting, abdominal pain, rheumatoid arthritis, etc.

l Kidney qi flank pain, wheezing and tingling: 50 grams of fresh fennel, mash and squeeze juice, add 50 ml of hot wine, and take it all at once.

2 Tinnitus caused by kidney deficiency: appropriate amount of fennel leaves, mash and extract juice, drip into the heart of the ear, drip on the right side for ringing, drip on the left side for ringing on the left side for ringing on the right side.

3 Malignant carbuncle: fennel, mash and squeeze juice 500 grams, take 3-4 times a day, and apply the residue to the affected area.

4 Rheumatic joint pain: 30 grams of fennel root, 30 grams of white soil Poria, stewed water for consumption.